{"id":303,"date":"2023-01-10T01:18:05","date_gmt":"2023-01-10T01:18:05","guid":{"rendered":"https:\/\/graywolfslair.com\/?p=303"},"modified":"2023-04-05T10:59:56","modified_gmt":"2023-04-05T10:59:56","slug":"9-4-12-thermos-extraction","status":"publish","type":"post","link":"https:\/\/graywolfslair.com\/index.php\/9-diy-cannamed-production\/9-4-extraction\/9-4-9-alkane-extraction\/9-4-12-thermos-extraction\/","title":{"rendered":"9.4.12 Thermos extraction"},"content":{"rendered":"\n<p class=\"wp-block-paragraph\">Jump117 shared an extraction technique with us on IC Mag forum, that used a stainless thermos to keep the LPG liquid longer, so as to increase residence time.&nbsp; To conduct our experiment, I first made a trip to Goodwill, where I picked up a couple stainless thermoses for about $8.00 each.<\/p>\n\n\n\n<p class=\"wp-block-paragraph\">My first step was to wash and sterilize the thermos, toss the screw cap, and to drill three holes in the cup covering the screw cap.&nbsp; I drilled one 1\/8\u201d hole in the center, and two 3\/16\u201d holes either side of center to allow fumes to vent.<\/p>\n\n\n\n<figure class=\"wp-block-image size-large\"><img loading=\"lazy\" decoding=\"async\" width=\"1024\" height=\"686\" src=\"https:\/\/graywolf.moveweight.com\/wp-content\/uploads\/2023\/04\/Drilled-cap-1024x686.webp\" alt=\"\" class=\"wp-image-1510\" srcset=\"https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Drilled-cap-1024x686.webp 1024w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Drilled-cap-300x201.webp 300w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Drilled-cap-768x514.webp 768w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Drilled-cap-1536x1028.webp 1536w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Drilled-cap-600x402.webp 600w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Drilled-cap-jpg.webp 1800w\" sizes=\"auto, (max-width: 1024px) 100vw, 1024px\" \/><\/figure>\n\n\n\n<p class=\"wp-block-paragraph\"><strong>Drilled cap<\/strong><\/p>\n\n\n\n<p class=\"wp-block-paragraph\">My next step was to accumulate the rest of my material and equipment, which besides the thermos included a can of lighter butane, a bain marie set, a strainer, and material to extract.&nbsp; Not shown is a cooler full of ice to store the butane in outdoors.<\/p>\n\n\n\n<figure class=\"wp-block-image\"><img decoding=\"async\" src=\"https:\/\/graywolf.moveweight.com\/images\/Equipment.jpg\" alt=\"\"\/><\/figure>\n\n\n\n<p class=\"wp-block-paragraph\"><strong>Equipment<\/strong><\/p>\n\n\n\n<p class=\"wp-block-paragraph\">Next step was to load the material to be extracted into the thermos, which we packed lightly and filled about \u00be\u2019s full.<\/p>\n\n\n\n<p class=\"wp-block-paragraph\">I then placed the thermos in the freezer at -18C\/0F and the butane into a cooler full of ice to chill overnight.&nbsp;<\/p>\n\n\n\n<p class=\"wp-block-paragraph\">I didn\u2019t put the butane in the freezer, because the valve seals lose resiliency as the temperature drops, and they are more prone to leaks, leading to possible explosions.<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><img loading=\"lazy\" decoding=\"async\" width=\"800\" height=\"536\" src=\"https:\/\/graywolf.moveweight.com\/wp-content\/uploads\/2023\/04\/Chilled-thermos-and-butane-jpg.webp\" alt=\"\" class=\"wp-image-1506\" srcset=\"https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Chilled-thermos-and-butane-jpg.webp 800w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Chilled-thermos-and-butane-300x201.webp 300w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Chilled-thermos-and-butane-768x515.webp 768w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Chilled-thermos-and-butane-600x402.webp 600w\" sizes=\"auto, (max-width: 800px) 100vw, 800px\" \/><\/figure>\n\n\n\n<p class=\"wp-block-paragraph\"><strong>Chilled thermos and butane<\/strong><\/p>\n\n\n\n<p class=\"wp-block-paragraph\">After selecting an ignition source free outdoor space with adequate airflow, the next step is to inject the chilled butane into the thermos through the center hole in the cap.<\/p>\n\n\n\n<figure class=\"wp-block-image size-large\"><img loading=\"lazy\" decoding=\"async\" width=\"1024\" height=\"686\" src=\"https:\/\/graywolf.moveweight.com\/wp-content\/uploads\/2023\/04\/Injecting-the-butane-1024x686.webp\" alt=\"\" class=\"wp-image-1507\" srcset=\"https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Injecting-the-butane-1024x686.webp 1024w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Injecting-the-butane-300x201.webp 300w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Injecting-the-butane-768x514.webp 768w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Injecting-the-butane-1536x1028.webp 1536w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Injecting-the-butane-600x402.webp 600w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Injecting-the-butane-jpg.webp 1800w\" sizes=\"auto, (max-width: 1024px) 100vw, 1024px\" \/><\/figure>\n\n\n\n<p class=\"wp-block-paragraph\"><strong>Injecting the butane<\/strong><\/p>\n\n\n\n<p class=\"wp-block-paragraph\">Once the thermos is full of butane, it is covered to insulate it and placed in a well ventilated shady spot to soak.&nbsp;<\/p>\n\n\n\n<figure class=\"wp-block-image\"><img decoding=\"async\" src=\"https:\/\/web.archive.org\/web\/20211026143118im_\/https:\/\/graywolf.moveweight.com\/images\/Soak_thermos.jpg\" alt=\"\"\/><\/figure>\n\n\n\n<p class=\"wp-block-paragraph\"><strong>Soaking<\/strong><\/p>\n\n\n\n<p class=\"wp-block-paragraph\">After a 10 minute soak, we rapidly drained the thermos by removing the cap and dumping the thermos inverted into the strainer, which we had sitting over the bain marie.<\/p>\n\n\n\n<figure class=\"wp-block-image\"><img decoding=\"async\" src=\"https:\/\/graywolf.moveweight.com\/images\/Dumping1.jpg\" alt=\"\"\/><\/figure>\n\n\n\n<p class=\"wp-block-paragraph\"><strong>Dumping<\/strong><\/p>\n\n\n\n<p class=\"wp-block-paragraph\">We then allowed the butane to boil away, aided by tap hot water in the lower bain marie container.<\/p>\n\n\n\n<figure class=\"wp-block-image\"><img decoding=\"async\" src=\"https:\/\/web.archive.org\/web\/20211026143118im_\/https:\/\/graywolf.moveweight.com\/images\/Boil_off.jpg\" alt=\"\"\/><\/figure>\n\n\n\n<p class=\"wp-block-paragraph\"><strong>Boiling off.<\/strong><\/p>\n\n\n\n<figure class=\"wp-block-image size-large\"><img loading=\"lazy\" decoding=\"async\" width=\"1024\" height=\"685\" src=\"https:\/\/graywolf.moveweight.com\/wp-content\/uploads\/2023\/04\/Yield-before-winterizing1-1024x685.webp\" alt=\"\" class=\"wp-image-1509\" srcset=\"https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Yield-before-winterizing1-1024x685.webp 1024w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Yield-before-winterizing1-300x201.webp 300w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Yield-before-winterizing1-768x514.webp 768w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Yield-before-winterizing1-600x402.webp 600w, https:\/\/graywolfslair.com\/wp-content\/uploads\/2023\/04\/Yield-before-winterizing1-jpg.webp 1200w\" sizes=\"auto, (max-width: 1024px) 100vw, 1024px\" \/><\/figure>\n\n\n\n<p class=\"wp-block-paragraph\"><strong>Yield from low grade trim before winterizing<\/strong><\/p>\n\n\n\n<p class=\"wp-block-paragraph\">Our last step was to add 190 proof ethanol to the bain marie and dissolve the extract at a ratio of about 10:1.&nbsp; That solution is then poured into a canning jar, sealed and placed in a -18C\/0F freezer for about 48 hours to precipitate the waxes, at which time it is filtered.&nbsp; See 10.2 Winterizing.<\/p>\n","protected":false},"excerpt":{"rendered":"<p>Jump117 shared an extraction technique with us on IC Mag forum, that used a stainless thermos to keep the LPG liquid longer, so as to [&hellip;]<\/p>\n","protected":false},"author":4,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[69],"tags":[],"class_list":["post-303","post","type-post","status-publish","format-standard","hentry","category-9-4-9-alkane-extraction"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v28.1 - https:\/\/yoast.com\/product\/yoast-seo-wordpress\/ -->\n<title>9.4.12 Thermos extraction - GrayWolf&#039;s Lair<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" 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