The optimum material from which to build an extractor system has to address chemical compatibility, strength of materials, and compliance to food service and pharmaceutical […]
15.21 How to make DIY Dry sieving frames
Dry sieve is a process by which the trichomes are broken off and sifted through a screen, allowing separation of the resin bearing trichomes from […]
15.20 The Grinning Reaper
I got my idea for the Grinning Reaper design, based on the short-lived Resin Reaper that briefly appeared in the market place, and Roger, a […]
15.19 Tumbling
Tumbling is a good way to process large amounts of material on the sidelines, while you occupy yourself with other chores or frolicking in play. […]
15.18 Electric nails
Easy to get spoiled by an electric nail! I know I sure have starting with the one mockup Growgeek and I assembled, which led Son […]
15.17 Induction heated nails
Induction heating has been around for a while and is used extensively to melt metal in foundries. The advantage is the rapid heat up and […]
15.16 Plant turnover and dipping fixture
One of my associates with a compromised immune system asked me to help her find an easier way to dip her plants for Spider Mites, […]
15.15 Distilling and Polishing LPG
For those of ya’ll with higher volume or whom need your Terpenators to stay on like pumping out concentrate, here is a design I did […]
15.14 DIY Vacuum chamber
Not only does a vacuum chamber or vacuum oven speed things up, but there are some things that you need one to accomplish. For those […]
15.13 Ethanol Subzero
For ya’ll brothers and sisters looking to process larger quantities at a time, we recommend that you consider the Subzero Ethanol process, by which either […]
15.12 Refurbishing a used Napco Vacuum Oven and Controls
For those of ya’ll coveting a vacuum oven on a limited budget, here is how we upgraded a used NAPCO 5851 vacuum drying oven to […]
15.11 Convert EXT-420 to selectable single or double stage operation
Haskel now offers their EXT-420 plumbed so that you can run it in either single or double stage, depending on where volume or pressure are […]
15.10 DIY Seed Separator
Here’s a real slick DIY seed separator shared with us by our UK brothers at Real Seeds: http://www.realseeds.co.uk/seedcleaner.html
15.9 Sanitary Clamp Pressure Ratings
For ya’ll that have been wondering what the different sanitary clamps are rated at, here is a handy chart. They are for you convenience only […]
15.8.1 Refluxing columns for producing 190 proof Ethanol
Still with 60″ packed Reflux column in operation In previous articles 10.19 190 Proof Ethanol from Scratch, and article 15.8 Ethanol Fractionating Still, I discus […]
15.8 Ethanol fractionating still
Ethanol is hygroscopic, so picks up water in the extraction process, and there are limits to how concentrated a pot still can keep keep the […]
15.7 Pot still
The simple pot still comes to us from simple roots buried in antiquity, but consists of a vessel that you can boil liquid in, and […]
15.6 ASME Pressure pots
Some of the professional engineering services certifying cannabis extraction equipment require that the collection pot have a certification placard attached and we’ve approached that a […]
15.5 The DIY Rotary Evaporator by Siskiyou Sam
Here is an article by Siskiyou Sam about a DYI rotary evaporator that he designed and built, and which he originally gave us permission to […]
15.4 The Evapanator DIY Rotary Thin Film Evaporator
Rotary evaporators are a keen thing to have if you’re running much alcohol, but alas the good ones are handsomely priced and finished material is not […]
15.3.3 Tri Coil Heat Exchanger Design
We used a couple different heat exchanger designs at WolfWurx, depending on application. One was the Tri Coil HEX, which we built ourselves using a […]
15.3.2 Counter flow heat exchangers
The other HEX design that we use is the counter flow design, which in our case is a 20′ 1/2″X .049 wall 304SS tube inside […]
15.3.1 Ethanol recovery heat exchanger
Here is a sweet little heat exchanger for recovering ethanol. I made it out of a stainless salad bowl, a bulk head fitting, and a […]
15.2 Lil Terp
During the time frame that I introduced the Mk III, I introduced the Lil Terp Passive extractor, which was based on the Mk III design, but […]
15.1 The History of the Terpenator According to Gospel
Success has many fathers, while failure is often a bastard child, so stories abound about how closed loop BHO extraction got started. Truth is also […]
10.19 190 Proof Ethanol from scratch
Legalization of medical cannabis has enabled brothers and sisters with limited funds to legally grow their own cannabis meds without the specter of arrest, but […]
10.18 Carbon Scrubbing & Diatomaceous Earth (DE) Filtering, by Ichiban Crafters
I ran across this article by Ichiban Crafter and Troy Ivan gave me permission to share it. More like it at Check out their site […]
10.17 Phytocanabinoids: a Unified Critical Inventory,
by Lumir Ondre Hanus, Stefan Martin Meyer, Eduardo Munoz, Orazio Taglialatela-Scafati and Giovanni Appendino Hee, hee, hee, here is a PDF link to an excellent […]
10.16 What are Anthocyanins
Anthocyanins are water soluble plant pigments known as polyphenols, a subgroup of flavonoids. They have a positive charge, which enables them to absorb light, and thus have colors, […]
10.15 Identifying cannabis strains by terpene profile
Here is an interesting open access paper on identifying cannabis strains by terpene profile by Doctor Justin Fischedick (Fis ched ik), 2020 EISohly awards winner […]
10.14 Plant Waxes
Plant waxes are the protective cover between the plant cells and their environment, by which they regulate their water loss, and protect themselves from the […]
10.13 Rate of THC Decomposition to CBN, et al
A reader recently brought CAT Scientific’s Debunking the Myth of THC-CBN Conversion Intensity study at https://www.catscientific.com/decarboxylating-cannabis/ to my attention, and asked my read, as it appeared to […]
10.12 Sustainable Production of Cannabinoids with Supercritical Carbon Dioxide Technologies
The following are some notes from the 212 page report by Hélène Perrotin-Brunel in the Netherlands, ISBN 978-90-8570-730-1, Copyright © 2011, Their copyright forbids copying, […]
10.11 Isolation of D9-THC from Hemp and analytical aspects
Isolation of D9-THC-a from hemp and analytical aspects concerning the determination of D9-THC in cannabis products, by Dussy, Hamberg, Luginbiihl, Schwerzmann, and Briellmann, from Institute […]
10.10 Alkanes and Alkane alcohols as solvents
Steam has been used for a couple hundred years to harvest the mono and sesquiterpenes, but by the time we reach the diterpenes, the boiling […]
10.9.1 Diamond Mining by Erich Berkovitz
Overview: Separating THCA and terpene fraction via evaporation crystallization Author Berkovitz with DIY Diamond Miner Example of Erich’s end product Steps: Pour Off: After running […]
10.9 THC-a Diamond Mining General Overview
Diamond mining refers to the practice of precipitating THC-a or CBD crystals out of a concentrated solution and starts with a subzero LPG extraction, typically […]
10.8.1 Introduction to Short Path Distillation, by Erich Berkovitz
Figure 1; My dirty old Chinese Short Path. This is a basic introduction to short path distillation of cannabinoids. We will be going over preparation […]
10.7.6 Opalene Silica Grandular Absorbent by Erich Berkovitz
Figure 1 Opaline Silica might just be the best thing since sliced bread. It is a granular absorbent containing hydrated silica (Amorphous Opaline Silica) and […]
10.7.5 Multicomponent Adsorption of Volatile Organic Compounds in the Liquid Phase: Predictive, Engineering Models, Molecular Simulations and Experiments.
Check out this study and paper done by C Brunch and published 2015 in Chemistry: https://pdfs.semanticscholar.org/b29b/a8094c8edd6d2dc58c33a983b55a77d8e626.pdf
10.7.4 ADSORBENT CLAYS, THEIR DISTRIBUTION, PROPERTIES PRODUCTION, AND USES
Your tax dollar at work! Here is an in depth article about adsorbent clays courtesy of US Geological Survey (USGS.gov). https://pubs.usgs.gov/bul/0928c/report.pdf
10.7.3 CRC 101, Intro to CRC and packing a poor man’s CRC
My name is Erich Berkovitz. I’ve been processing cannabis for about 10 years. I’ve been living in Oregon and an OMMP patient since 2013. For […]
10.7.2 CRC Murphy Murri style
One of the cannabis marketplace’s current blossoming love affairs is with color remediation chromatography (CRC). Actually, somewhat of a misnomer, in that chromatography simply separates […]
10.7.1 First Column Chromatography experiment
When packed into a column and solutions are passed through them, various media changes the rates that the different constituents in the solution reach the […]
10.6 Sweet Mary’s Charms III
Another thank you to Dr. Justin Fischedick for the pile-o-papers and studies, in support of my quest to solve the CBN riddle, and the study […]
10.5 THC-O-A Acetate
Disclaimer: The techniques described here require at least High School chemistry lab training and experience in chemistry lab techniques, as well as adequate ventilation and […]
10.4 Isomerizing
Disclaimer: The techniques described here require at least High School chemistry lab training and experience in chemistry lab techniques, as well as adequate ventilation and […]
10.3 Pentane/Hexane/Heptane and brine wash
Polishing Extract: We’ve discussed how to make pristine museum quality bragging rights concentrates, but what do you do after the fact, when what’cha got is […]
10.2 Winterizing
Winterizing is the term for redissolving a non polar extraction in a polar solvent and then lowering the temperature low and long enough for the […]
10.1.4 Decarboxylation 101
As produced by the cannabis plant, the cannabinoids are produced in carboxylic acid form, which means that there is a carboxyl group (COOH) attached. Note […]
10.1.3 Closed Wash Decarb by Ichiban Crafter
Hee, hee, hee, snicker, snark, snort! Check out this 150F Closed Wash Decarb paper by Ichiban Crafter!
10.1.2 Decarboxylating Ethanol Tinctures In Situ
One of the issues with extracting with ethanol and then using the alcohol mixture as a tincture, is that as extracted, THC-a does not readily […]
10.1.1 Decarboxylation of Tetrahydrocannabinolic acid (THCA) to active THC
10.1.1 Decarboxylation of Tetrahydrocannabinolic acid (THCA) to active THC by Iffland, Carus, Grotenhermen, at nova-Institute GmbH http://eiha.org/media/2014/08/16-10-25-Decarboxylation-of-THCA-to-active-THC.pdf Download this paper and further documents at: www.eiha.org This […]
10.1 Decarboxylation
As produced by the cannabis plant, the cannabinoids are produced in carboxylic acid form, which means that there is a carboxyl group (COOH) attached. Note […]
14.0 Resources
14.1 ASME Tanks 14.1.1 Marks Brothers 503-663-0211 marks-brothers.com 14.2 Books and links 14.2.1 Marijuana Chemistry, Michael Starks 14.2.2 Marijuana Gold-Trash to stash, Ed Rosenthal 14.2.3 Dr Atomic’s Marijuana […]
13.1 Certification
With legalization comes regulation, and a current one is that the extraction equipment and the operating system that it is installed in, must meet ASME, […]
12.1 Extraction Booth and Ventilation System Design
A certified and permitted extraction installation in OR, WA, CO, NV, and MD requires not only certified equipment, but an extraction booth that meets IBC, […]
9.5.9 Yet another way to vape without using e-pen carts
Some of us whose lungs are approaching their expiration date and who now rely on vaping or dabbing, are left wanting when traveling, so covet […]
9.5.8 Adabadoya snowballs
Royal Jelly certainly has smoothness and potency sorted out, but how about us’ns brothers and sisters that crave more monoterpene flavors? For ya’ll I have […]
9.5.7 Royal Jelly
I mixed some of Pharmer Joe’s center fraction Clear distillate and his THC-a crystals to make a delightful mix that we decided to call […]
9.5.6 Cannapops
I originally developed the Cannapop lollypops for Granny, a patient with jaw damage that left her with limited movement and constant pain. The lollypop allowed […]
9.5.5 Cannabuttons
Here’s a tale from the hoary days of yore, but one that still has brothers and sisters swearing by the product. In the olden days, […]
9.5.4 Dab and Vaporizations Sytems:
Most of us’ns first experience with cannabis was smoking it, but once its medical properties began to be better documented and medical cannabis came of […]
9.5.3 Suppositories
Aside from intravenous injections, the portals into the human body are oral, respiratory, transdermal, and rectal. For some applications like nausea and colon/rectal cancer, it […]
9.5.2 Graywolf’s EZ CBD Topical
Lu lu lu lu lu lu lu lu lu!!!!!!!!!! Now that’s pain relief from a Topical! This amazingly effective pain relieving topical is just too, […]
9.5.1 Holy Anointing Oil
Our Holy Anointing Oil oral/topical was formulated by Carla, aka Eloquentsolution, and was based on a recipe for Holy Anointing Oil give to Moses by the Lord […]
9.4.14.4 The Cotton Candy Extraction Technique
9.4.14.4 The Cotton Candy Extraction Technique We bumped into the Cotton Candy extraction technique by accident, while shaking out the original Mk III Terpenator. We […]
9.4.17 Extracting oil from fan leaves and stems
Sweet Mary not only has trichomes on her very special succulent parts, she has trichomes on both her fan leaves and her stems. Even her roots […]
9.4.16 Vacuum Purging
Heating a concentrate to its melting point in a vacuum oven or chamber, so as to reduce surface tension enough for bubbles to escape, and […]
9.4.14.3 The History of BHO
Success has many fathers, but failure is most often a bastard child. Lawrd knows who first conceived it, but who was the first to publish […]
9.4.14.2 Unloading Columns With Air
Unloading columns can be tedious and we experimented with various methods ranging from an auger and battery operated electric drill, but loved this one the […]
9.4.14.1 Vapor boost for cold injections
As the temperature of LPG drops, so does its pressure. The Engineering Tool Box offers a handy reference showing the pressure of different mixes at […]
9.4.13 Lil Terp Passive Extractor
During the time frame that I introduced the Mk III, I introduced the Lil Terp Passive extractor, which was based on the Mk III design, but […]
9.4.12 Thermos extraction
Jump117 shared an extraction technique with us on IC Mag forum, that used a stainless thermos to keep the LPG liquid longer, so as to […]
9.4.11 BHO Open Blast
BHO is the acronym for Butane Honey Oil, which is cannabis essential oils extracted using LPG as a solvent. That LPG typically contains n or […]
9.4.10 n-Butane, Isobutane, and Propane Rated GRAS by FDA
Flying in the face of the often espoused proffered opinion that any residual butane in your concentrate is “poison”, the Food and Drug Administration has […]
9.4.9.2.6 Mystery oil content by lighter fuel brand
Here is a rating of lighter fuel brands best to worst with regard to Mystery Oil content, as compiled by Skyhighler and offered at https://www.icmag.com/ic/showpost.php?p=6099306&postcount=28 Best […]
9.4.9.2.3 Butane Mystery Oil Removal using a Terpenator
Closed loop systems like the Terpenator also have the ability to vacuum distill the LPG used in the process, so as to reduce the PPM […]
9.4.9.2.2 Overview of BHO extraction
The target constituents in cannabis that we covet, are aromatic hydrocarbons soluble in the simple Alkanes n-Butane and n-Propane, as well as their isomers Isobutane […]
9.4.9.2.1 Butane Safety and social responsibility
Before we discuss extraction techniques, lets discuss safety and social responsibility. Butane and Propane are both high flammable and typically under pressure in their containers, […]
9.4.9.1 Pentane, Hexane, and Heptane simple Alkanes
Simple Alkane MSDS Sheets & Properties: The simple Alkanes most often involved in cannabis extraction are n-Propane, n-Butane, Isobutane, n-Pentane, n-Hexane. and n-Heptane. Their MSDS […]
9.4.8.1 QWISO
Quick Wash Isopropyl (QWISO) is similar to a QWET extraction using Ethanol, but uses cheaper un liquor taxed, 99% purity Isopropanol, found in places like […]
9.4.7.5 Recovery stills
Ethanol extraction is one of our favorite methods, especially when run size gets beyond practical size limits for LPG extraction, and high monoterpene retention isn’t […]
9.4.7.4 Alcohol Extraction Overview
Ethanol is one of the oldest solvents used to extract cannabis concentrates and due to its heavily taxed cost and hit and miss availability around […]
9.4.7.3 Giant Tea ball extraction
Giant Tea Ball Extraction A fast low tech way to extract a large amount of mixed trim fast, with a low equipment investment. Check out […]
9.4.7.2 Subzero extraction
9.4.7.2 Subzero Extraction For ya’ll brothers and sisters looking to process larger quantities at a time, we recommend that you consider the Subzero Ethanol process, […]
9.4.7.1 QWET
Quick Wash Ethanol is an extraction process by which we freeze the material and chill the Ethanol before extracting, so that we limit the pickup […]
9.4.6 Glycerol Extraction
Vegetable glycerin (glycerol) extraction is an easy effective way to extract cannabis concentrates, and within the capability of most folks to perform. It can be […]
9.4.5 Vegetable and Nut Oil Extraction
Sweet Mary’s terpenes, terpenoids, and cannabinoids dissolve readily in fats and oils, allowing us to use them (fats and oils) for both extraction, or simply […]
9.4.4 Rosin Extraction
So how about the new kid on the block Rosin! No solvents or license required. My best suggestion is to try it and decide for […]
9.4.2.2 Refining to full melt using electrostatic charges
Some of ya’ll are looking for a way to further refine heavily carded kif, and one way that works for small personal quantities, is electrostatic […]
9.4.2 Dry sieve
Kif comes from the Arabic kayf, meaning pleasure. While hand rubbed charas is ostensibly the oldest method of harvesting Kif, sieving does date back to […]
9.4.1 Hand rub Charas
Hand rubbed Charas is thought to be the oldest form of cannabis concentrate, predating sieving by centuries, if not eons. It is made by rubbing the […]
9.2.4 A crash course in grow room automation
By Pete Tewes, Aka GrowGeek IoT Integration Engineer Pt3 Technical, LLC. ***Full disclosure*** While I do happily work for a controls manufacture and have my […]