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GrayWolf's Lair

GrayWolf's Lair

A Posse ad Esse. From Possibility To Realization.

  • 1. About-Us
    • 1.1 Article by Graywolf/JD Ellis
    • 1.2 History and about
    • 1.3 The Grey Wolf in Alchemical symbology
    • 1.4 From Russia with love!
    • 1.5 Dr Kate Welch and our presentation at PSU
    • 1.6 What happened?
  • 2. Legal, Political, & Current Affairs
    • 2.1.1 Latest NORML Articles
    • 2.2 The Oil Wars
    • 2.4 Extraction Innovators U-tube regarding closed loop extraction evolution
  • 3. Medical
    • 3.1 Granny Storm Crow’s List 2019
    • 3.2 RIP Brandy
  • 4. Authors Columns
    • 4.1 Graywolf
      • 4.1.1 About JD aka Graywolf
      • 4.1.2 The Elvis(es) have left the building
      • 4.1.3 Posting standards for reader comments
      • 4.1.4 Process Evolution
      • 4.1.5 About 1.1’s new artwork by Dented Art
      • 4.1.7 Modern Extractor Bonus E02 POD cast with Graywolf.
      • 4.1.8 Where is this handbasket named Facebook headed??
      • 4.1.9 Thoughts and sayings
      • 4.1.10 New Nostalgic Book, by D. Gold
    • 4.2 Eloquent Solution
      • 4.2.1 About Carla Kay, Eloquent Solution
    • 4.3 Pharmer Joe
    • 4.4 Dr Kate Welch, Pharm D
      • 4.4.1 About Dr Kate Welch, Pharm D
      • 4.4.2 Cannabis Formula from the US Dispensatory, 1870
      • 4.4.3 Cannabinoid Carboxylic Acids, THCA and CBDA
      • 4.4.4 Introducing Dr Kate Welch, Pharm D
    • 4.6 D Gold
      • 4.6.1 About D Gold
      • 4.6.1.1 Hello and recollections, by D Gold
      • 4.6.2 Red oil in the late 60’s and early 70’s
      • 4.6.3 PURE THC for three bucks a gram?
      • 4.6.4 Dave Golds MEGAPLANT Challenge
      • 4.6.5 Questions About Long Term Flower Storage?? by Dave Gold
      • 4.6.6 The Chilum by Dave Gold
      • 4.6.7.Canna-Beer by D. Gold
        • 4.6.7.1 D Gold’s Cannabeer update
        • 4.6.7.2 A few more thoughts on CANNABEER by D Gold
        • 4.6.7.3 CO2 for cheap, beer for free by D Gold
      • 4.6.8 COVID, CBD, TERPENES, by D Gold
    • 4.7 Doug Cody
      • 4.7.2  The Solvent Wars, by Doug Cody, Cannabis Home Sciences
  • 5. Upcoming Speaker & Vendor Events
  • 6. Classes
  • 7. Raffles
  • 8. Essential Oil Safety
    • 8.1 Sweet Mary’s Charms
    • 8.2 Plant Waxes
    • 8.3 Salvaging Moldy Material
    • 8.4 Sweet Mary’s Charms II
    • 8.5 Oh Sweet Mary, What is that perfume you’re wearing?
    • 8.6 Where does all the color come from?
    • 8.7 Vaping illnesses and deaths
    • 8.8 Characterizing the smell of Marijuana by odor impact of volatile compounds
    • 8.9 Guide to buying Delta-8-THC, by Erich Berkovitz
    • 8.10 FDA Residual Solvent Standards
    • 8.11 Dr Justin Fischedick On Plant Terpenes
    • 8.12 Butane/Propane Mystery oil
    • 8.13 How much LPG mixture can I safely load in my tank?
    • 8.14 Please do not immolate yourselves extracting BHO Indoors
  • 9. DIY CannaMed Production
    • 9.1 Safety
      • 9.1.1 DIY Canna-med Production Safety
    • 9.2 Growing
      • 9.2.2 Indoor garden
      • 9.2.4 A crash course in grow room automation
    • 9.3 Harvesting Drying and Curing
    • 9.4 Extraction
      • 9.4.1 Hand rub Charas
      • 9.4.2 Dry sieve
        • 9.4.2.2 Refining to full melt using electrostatic charges
      • 9.4.3 Bubble
      • 9.4.4 Rosin Extraction
      • 9.4.5 Vegetable and Nut Oil Extraction
      • 9.4.6 Glycerol Extraction
      • 9.4.7 Ethanol extraction
        • 9.4.7.1 QWET
        • 9.4.7.2 Subzero extraction
        • 9.4.7.3 Giant Tea ball extraction
        • 9.4.7.4 Alcohol Extraction Overview
        • 9.4.7.5 Recovery stills
      • 9.4.8 Isopropyl extraction
        • 9.4.8.1 QWISO
      • 9.4.15 Pentane/Hexane/Heptane
      • 9.4.9 Alkane extraction
        • 9.4.9.1 Pentane, Hexane, and Heptane simple Alkanes
        • 9.4.9.2 Propane/Butane extractions
          • 9.4.9.2.1 Butane Safety and social responsibility
          • 9.4.9.2.2 Overview of BHO extraction
          • 9.4.9.2.3 Butane Mystery Oil Removal using a Terpenator
          • 9.4.9.2.6 Mystery oil content by lighter fuel brand
          • 9.4.9.3 Absolute Amber from Banana Silver Ladyboys by Jump117
      • 9.4.10 n-Butane, Isobutane, and Propane Rated GRAS by FDA
      • 9.4.11 BHO Open Blast
      • 9.4.12 Thermos extraction
      • 9.4.13 Lil Terp Passive Extractor
      • 9.4.14 Active Closed Loop
        • 9.4.14.1 Vapor boost for cold injections
        • 9.4.14.2 Unloading Columns With Air
        • 9.4.14.3 The History of BHO
      • 9.4.15 Pentane/Hexane/Heptane
        • 9.4.15.1 Extraction
        • 9.4.15.2 Recovery
      • 9.4.16 Vacuum Purging
      • 9.4.17 Extracting oil from fan leaves and stems
      • 9.4.14.4 The Cotton Candy Extraction Technique
    • 9.5 Formulation and Application
      • 9.5.1 Holy Anointing Oil
      • 9.5.2 Graywolf’s EZ CBD Topical
      • 9.5.3 Suppositories
      • 9.5.4 Dab and Vaporizations Sytems:
      • 9.5.5 Cannabuttons
      • 9.5.6 Cannapops
      • 9.5.7 Royal Jelly
      • 9.5.8 Adabadoya snowballs
      • 9.5.9 Yet another way to vape without using e-pen carts
  • 10. The Alchemist Resource
    • 10.1 Decarboxylation
      • 10.1.1 Decarboxylation of Tetrahydrocannabinolic acid (THCA) to active THC
      • 10.1.2 Decarboxylating Ethanol Tinctures In Situ
      • 10.1.3 Closed Wash Decarb by Ichiban Crafter
      • 10.1.4 Decarboxylation 101
    • 10.2 Winterizing
    • 10.3 Pentane/Hexane/Heptane and brine wash
    • 10.4 Isomerizing
    • 10.5 THC-O-A Acetate
    • 10.6 Sweet Mary’s Charms III
    • 10.7 CRC
      • 10.7.1 First Column Chromatography experiment
      • 10.7.2 CRC Murphy Murri style
      • 10.7.3 CRC 101, Intro to CRC and packing a poor man’s CRC
      • 10.7.4 ADSORBENT CLAYS, THEIR DISTRIBUTION, PROPERTIES PRODUCTION, AND USES
      • 10.7.5 Multicomponent Adsorption of Volatile Organic Compounds in the Liquid Phase: Predictive, Engineering Models, Molecular Simulations and Experiments.
      • 10.7.6 Opalene Silica Grandular Absorbent by Erich Berkovitz
    • 10.8 Short Path
      • 10.8.1 Introduction to Short Path Distillation, by Erich Berkovitz
    • 10.9 THC-a Diamond Mining General Overview
      • 10.9.1 Diamond Mining by Erich Berkovitz
    • 10.10 Alkanes and Alkane alcohols as solvents
    • 10.11 Isolation of D9-THC from Hemp and analytical aspects
    • 10.12 Sustainable Production of Cannabinoids with Supercritical Carbon Dioxide Technologies
    • 10.13 Rate of THC Decomposition to CBN, et al
    • 10.14 Plant Waxes
    • 10.15 Identifying cannabis strains by terpene profile
    • 10.16 What are Anthocyanins
    • 10.17 Phytocanabinoids: a Unified Critical Inventory,
    • 10.18 Carbon Scrubbing & Diatomaceous Earth (DE) Filtering, by Ichiban Crafters
    • 10.19 190 Proof Ethanol from scratch
  • 11. Commercial Processes
  • 12. Extraction Booth and Ventilation
    • 12.1 Extraction Booth and Ventilation System Design
  • 13. Certification
    • 13.1 Certification
  • 14. Resources
    • 14.0 Resources
  • 15. DIY Equipment
    • 15.1 The History of the Terpenator According to Gospel
    • 15.2 Lil Terp
    • 15.3 Heat exchangers
      • 15.3.1 Ethanol recovery heat exchanger
      • 15.3.2 Counter flow heat exchangers
      • 15.3.3 Tri Coil Heat Exchanger Design
    • 15.4 The Evapanator DIY Rotary Thin Film Evaporator
    • 15.5 The DIY Rotary Evaporator by Siskiyou Sam
    • 15.6 ASME Pressure pots
    • 15.7 Pot still
    • 15.8 Ethanol fractionating still
      • 15.8.1 Refluxing columns for producing 190 proof Ethanol
    • 15.9 Sanitary Clamp Pressure Ratings
    • 15.10 DIY Seed Separator
    • 15.11 Convert EXT-420 to selectable single or double stage operation
    • 15.12 Refurbishing a used Napco Vacuum Oven and Controls
    • 15.13 Ethanol Subzero
    • 15.14 DIY Vacuum chamber
    • 15.15 Distilling and Polishing LPG
    • 15.16 Plant turnover and dipping fixture
    • 15.17 Induction heated nails
    • 15.18 Electric nails
    • 15.19 Tumbling
    • 15.20 The Grinning Reaper
    • 15.21 How to make DIY Dry sieving frames
    • 15.22 Material choice for extractor systems
    • 15.23 Mk VIII Inline Dewaxing
    • 15.24 DIY SCFE CO2
    • 15.25 Hot vapor assist
    • 15.26 Acoustical Extraction
    • 15.27 Automating the Extraction Process
    • 15.28 Extractor Column Design
    • 15.29 Remediating spent BHO extraction material for residual solvent
    • 15.30 Behold the Mk III Evolution and ancillaries
    • 15.31 Let’s discuss universal pump laws!
    • 15.32 Cannabis Extraction Thermodynamics 101
  • 16. Commercial Equipment
    • 16.1 Producers columns
      • 16.1.1 ABM Equipment bulk cannabis drying system
      • 16.1.2 Lab Baths – the Good, the Bad, the Ugly
      • 16.1.3 DIRTY PURGE – Contamination Threats In Vacuum Purging
    • 16.2 Equipment tests
      • 16.2.1 Extract Craft Source Turbo
      • 16.2.2 Testing D Gold’s ISO-3
      • 16.2.3 HMI Titanium Skillet
      • 16.2.4 Evaluation of Heidolph Instruments Hei-VAP Precision ML G3
      • 16.2.5 Testing the CAT Scientific MCX-66 Stirring Hotplate
      • 16.2.6 Testing the Extract Craft EtOH Pro
      • 16.2.7 Field testing the Medxtract Essential
    • 16.3 Plant tours
      • 16.3.1 Subzero Scientific
  • 17.0 Used facilities and equipment for sale:
    • 17.1 An $8M industrial-scale, USDA-Certified CBD/THC distillate-making facility for $3.75M.
    • 17.2 Miscellaneous Processing Equipment
    • 17.3 More misc equipment from Sam
    • 17.4 More from Sam
    • 17.5 New stuff from Sam
    • 17.7 New stuff from Sam
    • 17.8 More goodies from Sam
    • 17.8 Used flash chromatography unit from Subzero Scientific
  • 18.0 The vacuum cooking and aluminum bead sous vide test sled
    • 18.0.1 The Vacuum Cooking and Aluminum Bead Sous Vide Test Sled, Chapter 2
    • 18.1 Sous Vide cooking with aluminum beads
      • 18.1.1 Aluminum Bead Crème Brulee Sous Vide
      • 18.1.2 Egg Bites
    • 18.3 Produce food concentrates extracting and boiling at low temperatures under vacuum
      • 18.3.1 Test 13 F-Extracting wild blackberry concentrates from spent pulp

Category: 10. The Alchemist Resource

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  • 10. The Alchemist Resource
  • 10. The Alchemist Resource

10.19 190 Proof Ethanol from scratch

Posted on January 10, 2023April 6, 2023 14 mins

Legalization of medical cannabis has enabled brothers and sisters with limited funds to legally grow their own cannabis meds without the specter of arrest, but […]

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  • 10. The Alchemist Resource

10.18 Carbon Scrubbing & Diatomaceous Earth (DE) Filtering, by Ichiban Crafters

Posted on January 10, 2023May 14, 2023 13 mins

I ran across this article by Ichiban Crafter and Troy Ivan gave me permission to share it.  More like it at Check out their site […]

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  • 10. The Alchemist Resource

10.17 Phytocanabinoids: a Unified Critical Inventory,

Posted on January 10, 2023March 21, 2023 1 min

by Lumir Ondre Hanus, Stefan Martin Meyer, Eduardo Munoz, Orazio Taglialatela-Scafati and Giovanni Appendino Hee, hee, hee, here is a PDF link to an excellent […]

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  • 10. The Alchemist Resource

10.16 What are Anthocyanins

Posted on January 10, 2023March 21, 2023 2 mins

Anthocyanins are water soluble plant pigments known as polyphenols, a subgroup of flavonoids.  They have a positive charge, which enables them to absorb light, and thus have colors, […]

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  • 10. The Alchemist Resource

10.15 Identifying cannabis strains by terpene profile

Posted on January 10, 2023May 14, 2023 2 mins

Here is an interesting open access paper on identifying cannabis strains by terpene profile by Doctor Justin Fischedick (Fis ched ik), 2020 EISohly awards winner […]

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  • 10. The Alchemist Resource

10.14 Plant Waxes

Posted on January 10, 2023March 21, 2023 3 mins

Plant waxes are the protective cover between the plant cells and their environment, by which they regulate their water loss, and protect themselves from the […]

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  • 10. The Alchemist Resource

10.13 Rate of THC Decomposition to CBN, et al

Posted on January 10, 2023April 6, 2023 5 mins

 A reader recently brought CAT Scientific’s Debunking the Myth of THC-CBN Conversion Intensity study at https://www.catscientific.com/decarboxylating-cannabis/ to my attention, and asked my read, as it appeared to […]

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  • 10. The Alchemist Resource

10.12 Sustainable Production of Cannabinoids with Supercritical Carbon Dioxide Technologies

Posted on January 10, 2023April 6, 2023 4 mins

The following are some notes from the 212 page report by Hélène Perrotin-Brunel in the Netherlands, ISBN 978-90-8570-730-1, Copyright © 2011, Their copyright forbids copying, […]

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  • 10. The Alchemist Resource

10.11 Isolation of D9-THC from Hemp and analytical aspects

Posted on January 10, 2023March 21, 2023 4 mins

Isolation of D9-THC-a from hemp and analytical aspects concerning the determination of D9-THC in cannabis products,   by Dussy, Hamberg, Luginbiihl, Schwerzmann, and Briellmann,  from Institute […]

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  • 10. The Alchemist Resource

10.10 Alkanes and Alkane alcohols as solvents

Posted on January 10, 2023April 6, 2023 13 mins

Steam has been used for a couple hundred years to harvest the mono and sesquiterpenes, but by the time we reach the diterpenes, the boiling […]

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  • 10. The Alchemist Resource

10.9.1 Diamond Mining by Erich Berkovitz

Posted on January 10, 2023March 21, 2023 9 mins

Overview: Separating THCA and terpene fraction via evaporation crystallization  Author Berkovitz with DIY Diamond Miner Example of Erich’s end product Steps: Pour Off: After running […]

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  • 10. The Alchemist Resource

10.9 THC-a Diamond Mining General Overview

Posted on January 10, 2023March 21, 2023 6 mins

Diamond mining refers to the practice of precipitating THC-a or CBD crystals out of a concentrated solution and starts with a subzero LPG extraction, typically […]

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  • 10.8 Short Path

10.8.1 Introduction to Short Path Distillation, by Erich Berkovitz

Posted on January 10, 2023April 6, 2023 23 mins

Figure 1; My dirty old Chinese Short Path. This is a basic introduction to short path distillation of cannabinoids. We will be going over preparation […]

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  • 10. The Alchemist Resource

10.8 Short Path

Posted on January 10, 2023March 21, 2023 0 mins
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  • 10.7 CRC

10.7.6 Opalene Silica Grandular Absorbent by Erich Berkovitz

Posted on January 10, 2023April 6, 2023 7 mins

Figure 1 Opaline Silica might just be the best thing since sliced bread. It is a granular absorbent containing hydrated silica (Amorphous Opaline Silica) and […]

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  • 10.7 CRC

10.7.5 Multicomponent Adsorption of Volatile Organic Compounds in the Liquid Phase: Predictive, Engineering Models, Molecular Simulations and Experiments.

Posted on January 10, 2023March 21, 2023 1 min

Check out this study and paper done by C Brunch and published 2015 in Chemistry: https://pdfs.semanticscholar.org/b29b/a8094c8edd6d2dc58c33a983b55a77d8e626.pdf

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  • 10.7 CRC

10.7.4 ADSORBENT CLAYS, THEIR DISTRIBUTION, PROPERTIES PRODUCTION, AND USES

Posted on January 10, 2023March 21, 2023 1 min

Your tax dollar at work!  Here is an in depth article about adsorbent clays courtesy of US Geological Survey (USGS.gov).   https://pubs.usgs.gov/bul/0928c/report.pdf

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  • 10.7 CRC

10.7.3 CRC 101, Intro to CRC and packing a poor man’s CRC

Posted on January 10, 2023March 21, 2023 10 mins

My name is Erich Berkovitz. I’ve been processing cannabis for about 10 years. I’ve been living in Oregon and an OMMP patient since 2013. For […]

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  • 10.7 CRC

10.7.2 CRC Murphy Murri style

Posted on January 10, 2023April 6, 2023 10 mins

One of the cannabis marketplace’s current blossoming love affairs is with color remediation chromatography (CRC).  Actually, somewhat of a misnomer, in that chromatography simply separates […]

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  • 10.7 CRC

10.7.1 First Column Chromatography experiment

Posted on January 10, 2023April 6, 2023 4 mins

When packed into a column and solutions are passed through them, various media changes the rates that the different constituents in the solution reach the […]

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  • 10. The Alchemist Resource

10.6 Sweet Mary’s Charms III

Posted on January 10, 2023March 21, 2023 3 mins

Another thank you to Dr. Justin Fischedick for the pile-o-papers and studies, in support of my quest to solve the CBN riddle, and the study […]

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  • 10. The Alchemist Resource

10.5 THC-O-A Acetate

Posted on January 10, 2023April 5, 2023 13 mins

Disclaimer:  The techniques described here require at least High School chemistry lab training and experience in chemistry lab techniques, as well as adequate ventilation and […]

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  • 10. The Alchemist Resource

10.4 Isomerizing

Posted on January 10, 2023April 5, 2023 7 mins

Disclaimer:  The techniques described here require at least High School chemistry lab training and experience in chemistry lab techniques, as well as adequate ventilation and […]

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  • 10. The Alchemist Resource

10.3 Pentane/Hexane/Heptane and brine wash

Posted on January 10, 2023April 4, 2023 8 mins

Polishing Extract: We’ve discussed how to make pristine museum quality bragging rights concentrates, but what do you do after the fact, when what’cha got is […]

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  • 10. The Alchemist Resource

10.2 Winterizing

Posted on January 10, 2023April 5, 2023 3 mins

Winterizing is the term for redissolving a non polar extraction in a polar solvent and then lowering the temperature low and long enough for the […]

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  • 10.1 Decarboxylation

10.1.4 Decarboxylation 101

Posted on January 10, 2023March 21, 2023 5 mins

As produced by the cannabis plant, the cannabinoids are produced in carboxylic acid form, which means that there is a carboxyl group (COOH) attached.  Note […]

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  • 10.1 Decarboxylation

10.1.3 Closed Wash Decarb by Ichiban Crafter

Posted on January 10, 2023March 21, 2023 1 min

Hee, hee, hee, snicker, snark, snort!  Check out this 150F Closed Wash Decarb paper by Ichiban Crafter!

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  • 10.1 Decarboxylation

10.1.2 Decarboxylating Ethanol Tinctures In Situ

Posted on January 10, 2023April 5, 2023 3 mins

One of the issues with extracting with ethanol and then using the alcohol mixture as a tincture, is that as extracted, THC-a does not readily […]

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  • 10.1 Decarboxylation

10.1.1 Decarboxylation of Tetrahydrocannabinolic acid (THCA) to active THC

Posted on January 10, 2023April 6, 2023 2 mins

10.1.1 Decarboxylation of Tetrahydrocannabinolic acid (THCA) to active THC by Iffland, Carus, Grotenhermen, at nova-Institute GmbH http://eiha.org/media/2014/08/16-10-25-Decarboxylation-of-THCA-to-active-THC.pdf Download this paper and further documents at: www.eiha.org  This […]

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  • 10. The Alchemist Resource

10.1 Decarboxylation

Posted on January 10, 2023March 21, 2023 5 mins

 As produced by the cannabis plant, the cannabinoids are produced in carboxylic acid form, which means that there is a carboxyl group (COOH) attached.  Note […]

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