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GrayWolf's Lair

GrayWolf's Lair

A Posse ad Esse. From Possibility To Realization.

  • 1. About-Us
    • 1.1 Article by Graywolf/JD Ellis
    • 1.2 History and about
    • 1.3 The Grey Wolf in Alchemical symbology
    • 1.4 From Russia with love!
    • 1.5 Dr Kate Welch and our presentation at PSU
    • 1.6 What happened?
  • 2. Legal, Political, & Current Affairs
    • 2.1.1 Latest NORML Articles
    • 2.2 The Oil Wars
    • 2.4 Extraction Innovators U-tube regarding closed loop extraction evolution
  • 3. Medical
    • 3.1 Granny Storm Crow’s List 2019
    • 3.2 RIP Brandy
  • 4. Authors Columns
    • 4.1 Graywolf
      • 4.1.1 About JD aka Graywolf
      • 4.1.2 The Elvis(es) have left the building
      • 4.1.3 Posting standards for reader comments
      • 4.1.4 Process Evolution
      • 4.1.5 About 1.1’s new artwork by Dented Art
      • 4.1.7 Modern Extractor Bonus E02 POD cast with Graywolf.
      • 4.1.8 Where is this handbasket named Facebook headed??
      • 4.1.9 Thoughts and sayings
      • 4.1.10 New Nostalgic Book, by D. Gold
    • 4.2 Eloquent Solution
      • 4.2.1 About Carla Kay, Eloquent Solution
    • 4.3 Pharmer Joe
    • 4.4 Dr Kate Welch, Pharm D
      • 4.4.1 About Dr Kate Welch, Pharm D
      • 4.4.2 Cannabis Formula from the US Dispensatory, 1870
      • 4.4.3 Cannabinoid Carboxylic Acids, THCA and CBDA
      • 4.4.4 Introducing Dr Kate Welch, Pharm D
    • 4.6 D Gold
      • 4.6.1 About D Gold
      • 4.6.1.1 Hello and recollections, by D Gold
      • 4.6.2 Red oil in the late 60’s and early 70’s
      • 4.6.3 PURE THC for three bucks a gram?
      • 4.6.4 Dave Golds MEGAPLANT Challenge
      • 4.6.5 Questions About Long Term Flower Storage?? by Dave Gold
      • 4.6.6 The Chilum by Dave Gold
      • 4.6.7.Canna-Beer by D. Gold
        • 4.6.7.1 D Gold’s Cannabeer update
        • 4.6.7.2 A few more thoughts on CANNABEER by D Gold
        • 4.6.7.3 CO2 for cheap, beer for free by D Gold
      • 4.6.8 COVID, CBD, TERPENES, by D Gold
    • 4.7 Doug Cody
      • 4.7.2  The Solvent Wars, by Doug Cody, Cannabis Home Sciences
  • 5. Upcoming Speaker & Vendor Events
  • 6. Classes
  • 7. Raffles
  • 8. Essential Oil Safety
    • 8.1 Sweet Mary’s Charms
    • 8.2 Plant Waxes
    • 8.3 Salvaging Moldy Material
    • 8.4 Sweet Mary’s Charms II
    • 8.5 Oh Sweet Mary, What is that perfume you’re wearing?
    • 8.6 Where does all the color come from?
    • 8.7 Vaping illnesses and deaths
    • 8.8 Characterizing the smell of Marijuana by odor impact of volatile compounds
    • 8.9 Guide to buying Delta-8-THC, by Erich Berkovitz
    • 8.10 FDA Residual Solvent Standards
    • 8.11 Dr Justin Fischedick On Plant Terpenes
    • 8.12 Butane/Propane Mystery oil
    • 8.13 How much LPG mixture can I safely load in my tank?
    • 8.14 Please do not immolate yourselves extracting BHO Indoors
  • 9. DIY CannaMed Production
    • 9.1 Safety
      • 9.1.1 DIY Canna-med Production Safety
    • 9.2 Growing
      • 9.2.2 Indoor garden
      • 9.2.4 A crash course in grow room automation
    • 9.3 Harvesting Drying and Curing
    • 9.4 Extraction
      • 9.4.1 Hand rub Charas
      • 9.4.2 Dry sieve
        • 9.4.2.2 Refining to full melt using electrostatic charges
      • 9.4.3 Bubble
      • 9.4.4 Rosin Extraction
      • 9.4.5 Vegetable and Nut Oil Extraction
      • 9.4.6 Glycerol Extraction
      • 9.4.7 Ethanol extraction
        • 9.4.7.1 QWET
        • 9.4.7.2 Subzero extraction
        • 9.4.7.3 Giant Tea ball extraction
        • 9.4.7.4 Alcohol Extraction Overview
        • 9.4.7.5 Recovery stills
      • 9.4.8 Isopropyl extraction
        • 9.4.8.1 QWISO
      • 9.4.15 Pentane/Hexane/Heptane
      • 9.4.9 Alkane extraction
        • 9.4.9.1 Pentane, Hexane, and Heptane simple Alkanes
        • 9.4.9.2 Propane/Butane extractions
          • 9.4.9.2.1 Butane Safety and social responsibility
          • 9.4.9.2.2 Overview of BHO extraction
          • 9.4.9.2.3 Butane Mystery Oil Removal using a Terpenator
          • 9.4.9.2.6 Mystery oil content by lighter fuel brand
          • 9.4.9.3 Absolute Amber from Banana Silver Ladyboys by Jump117
      • 9.4.10 n-Butane, Isobutane, and Propane Rated GRAS by FDA
      • 9.4.11 BHO Open Blast
      • 9.4.12 Thermos extraction
      • 9.4.13 Lil Terp Passive Extractor
      • 9.4.14 Active Closed Loop
        • 9.4.14.1 Vapor boost for cold injections
        • 9.4.14.2 Unloading Columns With Air
        • 9.4.14.3 The History of BHO
      • 9.4.15 Pentane/Hexane/Heptane
        • 9.4.15.1 Extraction
        • 9.4.15.2 Recovery
      • 9.4.16 Vacuum Purging
      • 9.4.17 Extracting oil from fan leaves and stems
      • 9.4.14.4 The Cotton Candy Extraction Technique
    • 9.5 Formulation and Application
      • 9.5.1 Holy Anointing Oil
      • 9.5.2 Graywolf’s EZ CBD Topical
      • 9.5.3 Suppositories
      • 9.5.4 Dab and Vaporizations Sytems:
      • 9.5.5 Cannabuttons
      • 9.5.6 Cannapops
      • 9.5.7 Royal Jelly
      • 9.5.8 Adabadoya snowballs
      • 9.5.9 Yet another way to vape without using e-pen carts
  • 10. The Alchemist Resource
    • 10.1 Decarboxylation
      • 10.1.1 Decarboxylation of Tetrahydrocannabinolic acid (THCA) to active THC
      • 10.1.2 Decarboxylating Ethanol Tinctures In Situ
      • 10.1.3 Closed Wash Decarb by Ichiban Crafter
      • 10.1.4 Decarboxylation 101
    • 10.2 Winterizing
    • 10.3 Pentane/Hexane/Heptane and brine wash
    • 10.4 Isomerizing
    • 10.5 THC-O-A Acetate
    • 10.6 Sweet Mary’s Charms III
    • 10.7 CRC
      • 10.7.1 First Column Chromatography experiment
      • 10.7.2 CRC Murphy Murri style
      • 10.7.3 CRC 101, Intro to CRC and packing a poor man’s CRC
      • 10.7.4 ADSORBENT CLAYS, THEIR DISTRIBUTION, PROPERTIES PRODUCTION, AND USES
      • 10.7.5 Multicomponent Adsorption of Volatile Organic Compounds in the Liquid Phase: Predictive, Engineering Models, Molecular Simulations and Experiments.
      • 10.7.6 Opalene Silica Grandular Absorbent by Erich Berkovitz
    • 10.8 Short Path
      • 10.8.1 Introduction to Short Path Distillation, by Erich Berkovitz
    • 10.9 THC-a Diamond Mining General Overview
      • 10.9.1 Diamond Mining by Erich Berkovitz
    • 10.10 Alkanes and Alkane alcohols as solvents
    • 10.11 Isolation of D9-THC from Hemp and analytical aspects
    • 10.12 Sustainable Production of Cannabinoids with Supercritical Carbon Dioxide Technologies
    • 10.13 Rate of THC Decomposition to CBN, et al
    • 10.14 Plant Waxes
    • 10.15 Identifying cannabis strains by terpene profile
    • 10.16 What are Anthocyanins
    • 10.17 Phytocanabinoids: a Unified Critical Inventory,
    • 10.18 Carbon Scrubbing & Diatomaceous Earth (DE) Filtering, by Ichiban Crafters
    • 10.19 190 Proof Ethanol from scratch
  • 11. Commercial Processes
  • 12. Extraction Booth and Ventilation
    • 12.1 Extraction Booth and Ventilation System Design
  • 13. Certification
    • 13.1 Certification
  • 14. Resources
    • 14.0 Resources
  • 15. DIY Equipment
    • 15.1 The History of the Terpenator According to Gospel
    • 15.2 Lil Terp
    • 15.3 Heat exchangers
      • 15.3.1 Ethanol recovery heat exchanger
      • 15.3.2 Counter flow heat exchangers
      • 15.3.3 Tri Coil Heat Exchanger Design
    • 15.4 The Evapanator DIY Rotary Thin Film Evaporator
    • 15.5 The DIY Rotary Evaporator by Siskiyou Sam
    • 15.6 ASME Pressure pots
    • 15.7 Pot still
    • 15.8 Ethanol fractionating still
      • 15.8.1 Refluxing columns for producing 190 proof Ethanol
    • 15.9 Sanitary Clamp Pressure Ratings
    • 15.10 DIY Seed Separator
    • 15.11 Convert EXT-420 to selectable single or double stage operation
    • 15.12 Refurbishing a used Napco Vacuum Oven and Controls
    • 15.13 Ethanol Subzero
    • 15.14 DIY Vacuum chamber
    • 15.15 Distilling and Polishing LPG
    • 15.16 Plant turnover and dipping fixture
    • 15.17 Induction heated nails
    • 15.18 Electric nails
    • 15.19 Tumbling
    • 15.20 The Grinning Reaper
    • 15.21 How to make DIY Dry sieving frames
    • 15.22 Material choice for extractor systems
    • 15.23 Mk VIII Inline Dewaxing
    • 15.24 DIY SCFE CO2
    • 15.25 Hot vapor assist
    • 15.26 Acoustical Extraction
    • 15.27 Automating the Extraction Process
    • 15.28 Extractor Column Design
    • 15.29 Remediating spent BHO extraction material for residual solvent
    • 15.30 Behold the Mk III Evolution and ancillaries
    • 15.31 Let’s discuss universal pump laws!
    • 15.32 Cannabis Extraction Thermodynamics 101
  • 16. Commercial Equipment
    • 16.1 Producers columns
      • 16.1.1 ABM Equipment bulk cannabis drying system
      • 16.1.2 Lab Baths – the Good, the Bad, the Ugly
      • 16.1.3 DIRTY PURGE – Contamination Threats In Vacuum Purging
    • 16.2 Equipment tests
      • 16.2.1 Extract Craft Source Turbo
      • 16.2.2 Testing D Gold’s ISO-3
      • 16.2.3 HMI Titanium Skillet
      • 16.2.4 Evaluation of Heidolph Instruments Hei-VAP Precision ML G3
      • 16.2.5 Testing the CAT Scientific MCX-66 Stirring Hotplate
      • 16.2.6 Testing the Extract Craft EtOH Pro
      • 16.2.7 Field testing the Medxtract Essential
    • 16.3 Plant tours
      • 16.3.1 Subzero Scientific
  • 17.0 Used facilities and equipment for sale:
    • 17.1 An $8M industrial-scale, USDA-Certified CBD/THC distillate-making facility for $3.75M.
    • 17.2 Miscellaneous Processing Equipment
    • 17.3 More misc equipment from Sam
    • 17.4 More from Sam
    • 17.5 New stuff from Sam
    • 17.7 New stuff from Sam
    • 17.8 More goodies from Sam
    • 17.8 Used flash chromatography unit from Subzero Scientific
  • 18.0 The vacuum cooking and aluminum bead sous vide test sled
    • 18.0.1 The Vacuum Cooking and Aluminum Bead Sous Vide Test Sled, Chapter 2
    • 18.1 Sous Vide cooking with aluminum beads
      • 18.1.1 Aluminum Bead Crème Brulee Sous Vide
      • 18.1.2 Egg Bites
    • 18.3 Produce food concentrates extracting and boiling at low temperatures under vacuum
      • 18.3.1 Test 13 F-Extracting wild blackberry concentrates from spent pulp

Category: 10.7 CRC

  • Home
  • Archive
  • 10. The Alchemist Resource
  • 10.7 CRC
  • 10.7 CRC

10.7.6 Opalene Silica Grandular Absorbent by Erich Berkovitz

Posted on January 10, 2023April 6, 2023 7 mins

Figure 1 Opaline Silica might just be the best thing since sliced bread. It is a granular absorbent containing hydrated silica (Amorphous Opaline Silica) and […]

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  • 10.7 CRC

10.7.5 Multicomponent Adsorption of Volatile Organic Compounds in the Liquid Phase: Predictive, Engineering Models, Molecular Simulations and Experiments.

Posted on January 10, 2023March 21, 2023 1 min

Check out this study and paper done by C Brunch and published 2015 in Chemistry: https://pdfs.semanticscholar.org/b29b/a8094c8edd6d2dc58c33a983b55a77d8e626.pdf

Read More
  • 10.7 CRC

10.7.4 ADSORBENT CLAYS, THEIR DISTRIBUTION, PROPERTIES PRODUCTION, AND USES

Posted on January 10, 2023March 21, 2023 1 min

Your tax dollar at work!  Here is an in depth article about adsorbent clays courtesy of US Geological Survey (USGS.gov).   https://pubs.usgs.gov/bul/0928c/report.pdf

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  • 10.7 CRC

10.7.3 CRC 101, Intro to CRC and packing a poor man’s CRC

Posted on January 10, 2023March 21, 2023 10 mins

My name is Erich Berkovitz. I’ve been processing cannabis for about 10 years. I’ve been living in Oregon and an OMMP patient since 2013. For […]

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  • 10.7 CRC

10.7.2 CRC Murphy Murri style

Posted on January 10, 2023April 6, 2023 10 mins

One of the cannabis marketplace’s current blossoming love affairs is with color remediation chromatography (CRC).  Actually, somewhat of a misnomer, in that chromatography simply separates […]

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  • 10.7 CRC

10.7.1 First Column Chromatography experiment

Posted on January 10, 2023April 6, 2023 4 mins

When packed into a column and solutions are passed through them, various media changes the rates that the different constituents in the solution reach the […]

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