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GrayWolf's Lair

GrayWolf's Lair

A Posse ad Esse. From Possibility To Realization.

  • 1. About-Us
    • 1.1 Article by Graywolf/JD Ellis
    • 1.2 History and about
    • 1.3 The Grey Wolf in Alchemical symbology
    • 1.4 From Russia with love!
    • 1.5 Dr Kate Welch and our presentation at PSU
    • 1.6 What happened?
  • 2. Legal, Political, & Current Affairs
    • 2.1.1 Latest NORML Articles
    • 2.2 The Oil Wars
    • 2.4 Extraction Innovators U-tube regarding closed loop extraction evolution
  • 3. Medical
    • 3.1 Granny Storm Crow’s List 2019
    • 3.2 RIP Brandy
  • 4. Authors Columns
    • 4.1 Graywolf
      • 4.1.1 About JD aka Graywolf
      • 4.1.2 The Elvis(es) have left the building
      • 4.1.3 Posting standards for reader comments
      • 4.1.4 Process Evolution
      • 4.1.5 About 1.1’s new artwork by Dented Art
      • 4.1.7 Modern Extractor Bonus E02 POD cast with Graywolf.
      • 4.1.8 Where is this handbasket named Facebook headed??
      • 4.1.9 Thoughts and sayings
      • 4.1.10 New Nostalgic Book, by D. Gold
    • 4.2 Eloquent Solution
      • 4.2.1 About Carla Kay, Eloquent Solution
    • 4.3 Pharmer Joe
    • 4.4 Dr Kate Welch, Pharm D
      • 4.4.1 About Dr Kate Welch, Pharm D
      • 4.4.2 Cannabis Formula from the US Dispensatory, 1870
      • 4.4.3 Cannabinoid Carboxylic Acids, THCA and CBDA
      • 4.4.4 Introducing Dr Kate Welch, Pharm D
    • 4.6 D Gold
      • 4.6.1 About D Gold
      • 4.6.1.1 Hello and recollections, by D Gold
      • 4.6.2 Red oil in the late 60’s and early 70’s
      • 4.6.3 PURE THC for three bucks a gram?
      • 4.6.4 Dave Golds MEGAPLANT Challenge
      • 4.6.5 Questions About Long Term Flower Storage?? by Dave Gold
      • 4.6.6 The Chilum by Dave Gold
      • 4.6.7.Canna-Beer by D. Gold
        • 4.6.7.1 D Gold’s Cannabeer update
        • 4.6.7.2 A few more thoughts on CANNABEER by D Gold
        • 4.6.7.3 CO2 for cheap, beer for free by D Gold
      • 4.6.8 COVID, CBD, TERPENES, by D Gold
    • 4.7 Doug Cody
      • 4.7.2  The Solvent Wars, by Doug Cody, Cannabis Home Sciences
  • 5. Upcoming Speaker & Vendor Events
  • 6. Classes
  • 7. Raffles
  • 8. Essential Oil Safety
    • 8.1 Sweet Mary’s Charms
    • 8.2 Plant Waxes
    • 8.3 Salvaging Moldy Material
    • 8.4 Sweet Mary’s Charms II
    • 8.5 Oh Sweet Mary, What is that perfume you’re wearing?
    • 8.6 Where does all the color come from?
    • 8.7 Vaping illnesses and deaths
    • 8.8 Characterizing the smell of Marijuana by odor impact of volatile compounds
    • 8.9 Guide to buying Delta-8-THC, by Erich Berkovitz
    • 8.10 FDA Residual Solvent Standards
    • 8.11 Dr Justin Fischedick On Plant Terpenes
    • 8.12 Butane/Propane Mystery oil
    • 8.13 How much LPG mixture can I safely load in my tank?
    • 8.14 Please do not immolate yourselves extracting BHO Indoors
  • 9. DIY CannaMed Production
    • 9.1 Safety
      • 9.1.1 DIY Canna-med Production Safety
    • 9.2 Growing
      • 9.2.2 Indoor garden
      • 9.2.4 A crash course in grow room automation
    • 9.3 Harvesting Drying and Curing
    • 9.4 Extraction
      • 9.4.1 Hand rub Charas
      • 9.4.2 Dry sieve
        • 9.4.2.2 Refining to full melt using electrostatic charges
      • 9.4.3 Bubble
      • 9.4.4 Rosin Extraction
      • 9.4.5 Vegetable and Nut Oil Extraction
      • 9.4.6 Glycerol Extraction
      • 9.4.7 Ethanol extraction
        • 9.4.7.1 QWET
        • 9.4.7.2 Subzero extraction
        • 9.4.7.3 Giant Tea ball extraction
        • 9.4.7.4 Alcohol Extraction Overview
        • 9.4.7.5 Recovery stills
      • 9.4.8 Isopropyl extraction
        • 9.4.8.1 QWISO
      • 9.4.15 Pentane/Hexane/Heptane
      • 9.4.9 Alkane extraction
        • 9.4.9.1 Pentane, Hexane, and Heptane simple Alkanes
        • 9.4.9.2 Propane/Butane extractions
          • 9.4.9.2.1 Butane Safety and social responsibility
          • 9.4.9.2.2 Overview of BHO extraction
          • 9.4.9.2.3 Butane Mystery Oil Removal using a Terpenator
          • 9.4.9.2.6 Mystery oil content by lighter fuel brand
          • 9.4.9.3 Absolute Amber from Banana Silver Ladyboys by Jump117
      • 9.4.10 n-Butane, Isobutane, and Propane Rated GRAS by FDA
      • 9.4.11 BHO Open Blast
      • 9.4.12 Thermos extraction
      • 9.4.13 Lil Terp Passive Extractor
      • 9.4.14 Active Closed Loop
        • 9.4.14.1 Vapor boost for cold injections
        • 9.4.14.2 Unloading Columns With Air
        • 9.4.14.3 The History of BHO
      • 9.4.15 Pentane/Hexane/Heptane
        • 9.4.15.1 Extraction
        • 9.4.15.2 Recovery
      • 9.4.16 Vacuum Purging
      • 9.4.17 Extracting oil from fan leaves and stems
      • 9.4.14.4 The Cotton Candy Extraction Technique
    • 9.5 Formulation and Application
      • 9.5.1 Holy Anointing Oil
      • 9.5.2 Graywolf’s EZ CBD Topical
      • 9.5.3 Suppositories
      • 9.5.4 Dab and Vaporizations Sytems:
      • 9.5.5 Cannabuttons
      • 9.5.6 Cannapops
      • 9.5.7 Royal Jelly
      • 9.5.8 Adabadoya snowballs
      • 9.5.9 Yet another way to vape without using e-pen carts
  • 10. The Alchemist Resource
    • 10.1 Decarboxylation
      • 10.1.1 Decarboxylation of Tetrahydrocannabinolic acid (THCA) to active THC
      • 10.1.2 Decarboxylating Ethanol Tinctures In Situ
      • 10.1.3 Closed Wash Decarb by Ichiban Crafter
      • 10.1.4 Decarboxylation 101
    • 10.2 Winterizing
    • 10.3 Pentane/Hexane/Heptane and brine wash
    • 10.4 Isomerizing
    • 10.5 THC-O-A Acetate
    • 10.6 Sweet Mary’s Charms III
    • 10.7 CRC
      • 10.7.1 First Column Chromatography experiment
      • 10.7.2 CRC Murphy Murri style
      • 10.7.3 CRC 101, Intro to CRC and packing a poor man’s CRC
      • 10.7.4 ADSORBENT CLAYS, THEIR DISTRIBUTION, PROPERTIES PRODUCTION, AND USES
      • 10.7.5 Multicomponent Adsorption of Volatile Organic Compounds in the Liquid Phase: Predictive, Engineering Models, Molecular Simulations and Experiments.
      • 10.7.6 Opalene Silica Grandular Absorbent by Erich Berkovitz
    • 10.8 Short Path
      • 10.8.1 Introduction to Short Path Distillation, by Erich Berkovitz
    • 10.9 THC-a Diamond Mining General Overview
      • 10.9.1 Diamond Mining by Erich Berkovitz
    • 10.10 Alkanes and Alkane alcohols as solvents
    • 10.11 Isolation of D9-THC from Hemp and analytical aspects
    • 10.12 Sustainable Production of Cannabinoids with Supercritical Carbon Dioxide Technologies
    • 10.13 Rate of THC Decomposition to CBN, et al
    • 10.14 Plant Waxes
    • 10.15 Identifying cannabis strains by terpene profile
    • 10.16 What are Anthocyanins
    • 10.17 Phytocanabinoids: a Unified Critical Inventory,
    • 10.18 Carbon Scrubbing & Diatomaceous Earth (DE) Filtering, by Ichiban Crafters
    • 10.19 190 Proof Ethanol from scratch
  • 11. Commercial Processes
  • 12. Extraction Booth and Ventilation
    • 12.1 Extraction Booth and Ventilation System Design
  • 13. Certification
    • 13.1 Certification
  • 14. Resources
    • 14.0 Resources
  • 15. DIY Equipment
    • 15.1 The History of the Terpenator According to Gospel
    • 15.2 Lil Terp
    • 15.3 Heat exchangers
      • 15.3.1 Ethanol recovery heat exchanger
      • 15.3.2 Counter flow heat exchangers
      • 15.3.3 Tri Coil Heat Exchanger Design
    • 15.4 The Evapanator DIY Rotary Thin Film Evaporator
    • 15.5 The DIY Rotary Evaporator by Siskiyou Sam
    • 15.6 ASME Pressure pots
    • 15.7 Pot still
    • 15.8 Ethanol fractionating still
      • 15.8.1 Refluxing columns for producing 190 proof Ethanol
    • 15.9 Sanitary Clamp Pressure Ratings
    • 15.10 DIY Seed Separator
    • 15.11 Convert EXT-420 to selectable single or double stage operation
    • 15.12 Refurbishing a used Napco Vacuum Oven and Controls
    • 15.13 Ethanol Subzero
    • 15.14 DIY Vacuum chamber
    • 15.15 Distilling and Polishing LPG
    • 15.16 Plant turnover and dipping fixture
    • 15.17 Induction heated nails
    • 15.18 Electric nails
    • 15.19 Tumbling
    • 15.20 The Grinning Reaper
    • 15.21 How to make DIY Dry sieving frames
    • 15.22 Material choice for extractor systems
    • 15.23 Mk VIII Inline Dewaxing
    • 15.24 DIY SCFE CO2
    • 15.25 Hot vapor assist
    • 15.26 Acoustical Extraction
    • 15.27 Automating the Extraction Process
    • 15.28 Extractor Column Design
    • 15.29 Remediating spent BHO extraction material for residual solvent
    • 15.30 Behold the Mk III Evolution and ancillaries
    • 15.31 Let’s discuss universal pump laws!
    • 15.32 Cannabis Extraction Thermodynamics 101
  • 16. Commercial Equipment
    • 16.1 Producers columns
      • 16.1.1 ABM Equipment bulk cannabis drying system
      • 16.1.2 Lab Baths – the Good, the Bad, the Ugly
      • 16.1.3 DIRTY PURGE – Contamination Threats In Vacuum Purging
    • 16.2 Equipment tests
      • 16.2.1 Extract Craft Source Turbo
      • 16.2.2 Testing D Gold’s ISO-3
      • 16.2.3 HMI Titanium Skillet
      • 16.2.4 Evaluation of Heidolph Instruments Hei-VAP Precision ML G3
      • 16.2.5 Testing the CAT Scientific MCX-66 Stirring Hotplate
      • 16.2.6 Testing the Extract Craft EtOH Pro
      • 16.2.7 Field testing the Medxtract Essential
    • 16.3 Plant tours
      • 16.3.1 Subzero Scientific
  • 17.0 Used facilities and equipment for sale:
    • 17.1 An $8M industrial-scale, USDA-Certified CBD/THC distillate-making facility for $3.75M.
    • 17.2 Miscellaneous Processing Equipment
    • 17.3 More misc equipment from Sam
    • 17.4 More from Sam
    • 17.5 New stuff from Sam
    • 17.7 New stuff from Sam
    • 17.8 More goodies from Sam
    • 17.8 Used flash chromatography unit from Subzero Scientific
  • 18.0 The vacuum cooking and aluminum bead sous vide test sled
    • 18.0.1 The Vacuum Cooking and Aluminum Bead Sous Vide Test Sled, Chapter 2
    • 18.1 Sous Vide cooking with aluminum beads
      • 18.1.1 Aluminum Bead Crème Brulee Sous Vide
      • 18.1.2 Egg Bites
    • 18.3 Produce food concentrates extracting and boiling at low temperatures under vacuum
      • 18.3.1 Test 13 F-Extracting wild blackberry concentrates from spent pulp

Category: 15. DIY Equipment

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  • Archive
  • 15. DIY Equipment
  • 15. DIY Equipment

15.32 Cannabis Extraction Thermodynamics 101

Posted on January 11, 2023March 21, 2023 38 mins

Now that more brothers and sisters are using closed loop LPG and EtOH extraction systems at subzero temperatures, questions regularly arise as to how much […]

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  • 15. DIY Equipment

15.31 Let’s discuss universal pump laws!

Posted on January 11, 2023January 11, 2023 6 mins

There is a lot of discussion about which recovery pump is best suited for our application and my first thought is to ask which one […]

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  • 15. DIY Equipment

15.30 Behold the Mk III Evolution and ancillaries

Posted on January 11, 2023April 6, 2023 6 mins

While I first shared the Terpenator design on 2-7-2011 on both SPR and IC Mag, and subsequently the fully automated Mk II, it was really […]

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  • 15. DIY Equipment

15.29 Remediating spent BHO extraction material for residual solvent

Posted on January 11, 2023January 11, 2023 2 mins

In answering process questions via email or at other forums, one cropped up that I thought I might share.  That was how do you process […]

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  • 15. DIY Equipment

15.28 Extractor Column Design

Posted on January 11, 2023April 6, 2023 6 mins

A discussion of extraction column design would not be complete without first discussing subzero extraction.  As the LPG cannabis extraction process has evolved, we’ve learned […]

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  • 15. DIY Equipment

15.27 Automating the Extraction Process

Posted on January 11, 2023May 15, 2023 12 mins

I recently got a call querying the details of how we automated the extraction process on the WolfWurx Mk VA2’s, but the story actually predates […]

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  • 15. DIY Equipment

15.26 Acoustical Extraction

Posted on January 11, 2023April 5, 2023 3 mins

Besides the highly individualized hand jive style of extraction using a screen, the question arises as to how much support we might expect from music, […]

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  • 15. DIY Equipment

15.23 Mk VIII Inline Dewaxing

Posted on January 11, 2023April 5, 2023 2 mins

There are a couple divergent lines of thinking with regard to BHO extraction.  In Plan A, we chill the LPG low enough to minimize plant […]

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  • 15. DIY Equipment

15.25 Hot vapor assist

Posted on January 11, 2023January 11, 2023 3 mins

As the temperature of LPG drops, so does its pressure.  The Engineering Tool Box offers a handy reference showing the pressure of different mixes at […]

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  • 15. DIY Equipment

15.24 DIY SCFE CO2

Posted on January 11, 2023May 15, 2023 34 mins

Sooooooo, why not passive SCFE CO2 extraction!  The sabriousness of CO2 certainly makes it attractive, and C02 becomes supercritical at only about 31C/87.8F at 1073 […]

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  • 15. DIY Equipment

15.22 Material choice for extractor systems

Posted on January 10, 2023January 11, 2023 6 mins

The optimum material from which to build an extractor system has to address chemical compatibility, strength of materials, and compliance to food service and pharmaceutical […]

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  • 15. DIY Equipment

15.21 How to make DIY Dry sieving frames

Posted on January 10, 2023May 15, 2023 16 mins

Dry sieve is a process by which the trichomes are broken off and sifted through a screen, allowing separation of the resin bearing trichomes from […]

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  • 15. DIY Equipment

15.20 The Grinning Reaper

Posted on January 10, 2023May 15, 2023 3 mins

I got my idea for the Grinning Reaper design, based on the short-lived Resin Reaper that briefly appeared in the market place, and Roger, a […]

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  • 15. DIY Equipment

15.19 Tumbling

Posted on January 10, 2023April 5, 2023 5 mins

Tumbling is a good way to process large amounts of material on the sidelines, while you occupy yourself with other chores or frolicking in play.  […]

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  • 15. DIY Equipment

15.18 Electric nails

Posted on January 10, 2023May 15, 2023 3 mins

Easy to get spoiled by an electric nail!  I know I sure have starting with the one mockup Growgeek and I assembled, which led Son […]

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  • 15. DIY Equipment

15.17 Induction heated nails

Posted on January 10, 2023May 15, 2023 2 mins

Induction heating has been around for a while and is used extensively to melt metal in foundries.  The advantage is the rapid heat up and […]

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  • 15. DIY Equipment

15.16 Plant turnover and dipping fixture

Posted on January 10, 2023April 5, 2023 2 mins

 One of my associates with a compromised immune system asked me to help her find an easier way to dip her plants for Spider Mites, […]

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  • 15. DIY Equipment

15.15 Distilling and Polishing LPG

Posted on January 10, 2023April 5, 2023 1 min

For those of ya’ll with higher volume or whom need your Terpenators to stay on like pumping out concentrate, here is a design I did […]

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  • 15. DIY Equipment

15.14 DIY Vacuum chamber

Posted on January 10, 2023May 15, 2023 9 mins

Not only does a vacuum chamber or vacuum oven speed things up, but there are some things that you need one to accomplish.  For those […]

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  • 15. DIY Equipment

15.13 Ethanol Subzero

Posted on January 10, 2023April 5, 2023 2 mins

For ya’ll brothers and sisters looking to process larger quantities at a time, we recommend that you consider the Subzero Ethanol process, by which either […]

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  • 15. DIY Equipment

15.12 Refurbishing a used Napco Vacuum Oven and Controls

Posted on January 10, 2023April 5, 2023 5 mins

For those of ya’ll coveting a vacuum oven on a limited budget, here is how we upgraded a used NAPCO 5851 vacuum drying oven to […]

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  • 15. DIY Equipment

15.11 Convert EXT-420 to selectable single or double stage operation

Posted on January 10, 2023April 5, 2023 1 min

Haskel now offers their EXT-420 plumbed so that you can run it in either single or double stage, depending on where volume or pressure are […]

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  • 15. DIY Equipment

15.10 DIY Seed Separator

Posted on January 10, 2023May 15, 2023 1 min

 Here’s a real slick DIY seed separator shared with us by our UK brothers at Real Seeds: http://www.realseeds.co.uk/seedcleaner.html

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  • 15. DIY Equipment

15.9 Sanitary Clamp Pressure Ratings

Posted on January 10, 2023March 21, 2023 2 mins

For ya’ll that have been wondering what the different sanitary clamps are rated at, here is a handy chart.  They are for you convenience only […]

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  • 15.8 Ethanol fractionating still

15.8.1 Refluxing columns for producing 190 proof Ethanol

Posted on January 10, 2023April 5, 2023 5 mins

Still with 60″ packed Reflux column in operation In previous articles 10.19 190 Proof Ethanol from Scratch, and article 15.8 Ethanol Fractionating Still, I discus […]

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  • 15. DIY Equipment

15.8 Ethanol fractionating still

Posted on January 10, 2023April 5, 2023 7 mins

Ethanol is hygroscopic, so picks up water in the extraction process, and there are limits to how concentrated a pot still can keep keep the […]

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  • 15. DIY Equipment

15.7 Pot still

Posted on January 10, 2023April 5, 2023 2 mins

The simple pot still comes to us from simple roots buried in antiquity, but consists of a vessel that you can boil liquid in, and […]

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  • 15. DIY Equipment

15.6 ASME Pressure pots

Posted on January 10, 2023May 15, 2023 6 mins

Some of the professional engineering services certifying cannabis extraction equipment require that the collection pot have a certification placard attached and we’ve approached that a […]

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  • 15. DIY Equipment

15.5 The DIY Rotary Evaporator by Siskiyou Sam

Posted on January 10, 2023March 21, 2023 3 mins

Here is an article by Siskiyou Sam about a DYI rotary evaporator that he designed and built, and which he originally gave us permission to […]

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  • 15. DIY Equipment

15.4 The Evapanator DIY Rotary Thin Film Evaporator

Posted on January 10, 2023April 5, 2023 2 mins

Rotary evaporators are a keen thing to have if you’re running much alcohol, but alas the good ones are handsomely priced and finished material is not […]

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  • 15.3 Heat exchangers

15.3.3 Tri Coil Heat Exchanger Design

Posted on January 10, 2023April 5, 2023 3 mins

We used a couple different heat exchanger designs at WolfWurx, depending on application.  One was the Tri Coil HEX, which we built ourselves using a […]

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  • 15.3 Heat exchangers

15.3.2 Counter flow heat exchangers

Posted on January 10, 2023March 21, 2023 2 mins

 The other HEX design that we use is the counter flow design, which in our case is a 20′ 1/2″X .049 wall 304SS tube inside […]

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  • 15.3 Heat exchangers

15.3.1 Ethanol recovery heat exchanger

Posted on January 10, 2023April 5, 2023 1 min

Here is a sweet little heat exchanger for recovering ethanol.  I made it out of a stainless salad bowl, a bulk head fitting, and a […]

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  • 15. DIY Equipment

15.2 Lil Terp

Posted on January 10, 2023April 5, 2023 4 mins

During the time frame that I introduced the Mk III, I introduced the Lil Terp Passive extractor, which was based on the Mk III design, but […]

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  • 15. DIY Equipment

15.1 The History of the Terpenator According to Gospel

Posted on January 10, 2023May 15, 2023 28 mins

Success has many fathers, while failure is often a bastard child, so stories abound about how closed loop BHO extraction got started.  Truth is also […]

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